In　order　to　realize　the　rapid,　nondestructive　detection　of　organic　compounds,　a　two-dimensional　analysis　method　based　on　technology　of　laser　Raman　spectroscopy　was　proposed.　The　results　show　that　using　532　nm　laser　as　excitation　light　source,　the　observation　of　236.2,　348.9,　449.4　and　513.6　cm-1,　the　four　vibrational　Raman　spectra,　and　the　intensity　ratio　of　6.4:1.7:9.4:1.0　can　determine　the　existence　of　tetrachloroethylene.　The　observation　of　707.5,　1　087.9,　1　175.8　and　3　078.6　cm-1,　the　four　vibrational　Raman　spectra,　and　the　intensity　ratio　of　9.6:6.4:1.0:3.9　can　determine　the　existence　of　chlorobenzene.　In　other　words,　that　through　the　comprehensive　study　of　spectral　lines　and　intensity　ratio　of　some　spectral　lines,　the　presence　of　organic　compounds　in　the　mixed　solution　can　be　determined　quickly.　In　the　aspect　of　quantitative　analysis,　using　multi-spectral　analysis　combined　with　least　square　fitting　method　can　improve　the　reliability　of　the　measurement,　The　accuracy　of　sample　concentration　was　98.4%.　This　spectral　measurement　method　is　a　potential　tool　for　organic　component　identification　and　concentration　analysis　which　has　a　prosperous　application　prospects.