The synthesis and crystal structure of a copper-sulfur cluster [Cu4(S5)2(C5H5N)4]·S8 - Details

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author：

Li, H. (Li, H..) ^[1] | Sheng, T. (Sheng, T..) ^[2] | Huang, Q. (Huang, Q..) ^[3] | Wu, X. (Wu, X..) ^[4]

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Abstract：

The　cluster　[Cu4(S5)2(C5H5N)4]·S8　with　cage　structure　has　been　obtained　by　reaction　of　copper　powder　with　sulfur　and　K2Sx　in　pyridine,　and　its　structure　was　determined　by　X-ray　crystallography.　The　crystal　data　for　the　title　compound:　triclinic,　P　{Mathematical　expression}　(No.　2),　Z　=　2,　a　=　11.818(4)　Å,　b　=　13.155(3)　Å,　c　=　14.177(4)　Å,　α　=　93.79(2)°,　β　=　96.68(2)°,　γ　=　115.76(2)°,　V　=　1954.52(1)　Å3.　The　structure　was　refined　to　R　=　0.038　Rw　=　0.053)　for　6444　data　with　I　>　3.0σ(I).　©　1995　Plenum　Publishing　Corporation.

Keyword：

cluster; copper-sulfur; Structure

Community：

[ 1 ] [Li, H.]Department of Chemistry, Fuzhou University, Fuzhou, Fujian, 350002, China
[ 2 ] [Sheng, T.]State Key Laboratory of Structure Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China
[ 3 ] [Huang, Q.]State Key Laboratory of Structure Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China
[ 4 ] [Wu, X.]State Key Laboratory of Structure Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China

Reprint 's Address：

[Wu, X.]State Key Laboratory of Structure Chemistry, Fujian Institute of Research on the Structure of Matter, Chinese Academy of Sciences, Fuzhou, Fujian, 350002, China

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Source ：

Journal of Cluster Science

ISSN： 1040-7278

Year： 1995

Issue： 3

Volume： 6

Page： 403-410

2 . 7 0 0

JCR@2023

ESI Discipline： CHEMISTRY;

Cited Count：

WoS CC Cited Count：

SCOPUS Cited Count： 5

ESI Highly Cited Papers on the List： 0 Unfold All

WanFang Cited Count：

Chinese Cited Count：

30 Days PV： 2

Affiliated Colleges：

化学化工学院本学院/部未明确归属的数据

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