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author:

Li, Yanwen (Li, Yanwen.) [1] | Xiang, Congying (Xiang, Congying.) [2] | Su, Xiaohui (Su, Xiaohui.) [3] | Li, Siwei (Li, Siwei.) [4] | Gu, Hui (Gu, Hui.) [5] | Luo, Jian (Luo, Jian.) [6] | Yin, Xiaowei (Yin, Xiaowei.) [7] | Yu, Zhiyang (Yu, Zhiyang.) [8] (Scholars:喻志阳)

Indexed by:

EI Scopus SCIE

Abstract:

The understanding of the microstructures is critical to the design of SiC fibers with excellent thermal stability and mechanical properties. We introduce a density-sensitive electron microscopy method, high-angle annular dark field (HAADF) imaging to study the microstructure of SiC fibers processed at a variety of temperatures ranging from 1200 to 1800 degrees C. It is revealed that, irrespective of their processing temperatures, SiC grains form the skeleton of SiC fibers that are surrounded by a multiple of zones with low HAADF contrast (low-density zones, LDZs). LDZs mainly consist of amorphous SiOC phases and turbostratic graphite. As a result, three important interfaces that dictate grain growth, namely, the SiC/amorphous SiOC interface, the SiC/turbostratic graphite phase boundary and the SiC high angle grain boundary (HAGBs) emerge. We find that, the SiC/turbostratic graphite interfaces and the SiC HAGBs are more effective in suppressing the growth of SiC grains than the SiC/a-SiOC interfaces on a basis of extensive TEM characterization. Aberration corrected TEM reveals marked differences in the atomic structures of those three interfaces, shedding light on how the interfacial structures affect grain growth of SiC fibers.

Keyword:

Electron microscopy Grain growth Interfacial structure Microstructure SiC fiber

Community:

  • [ 1 ] [Li, Yanwen]Fuzhou Univ, Coll Chem, State Key Lab Photocatalysis Energy & Environm, Fuzhou 350002, Peoples R China
  • [ 2 ] [Xiang, Congying]Fuzhou Univ, Coll Chem, State Key Lab Photocatalysis Energy & Environm, Fuzhou 350002, Peoples R China
  • [ 3 ] [Yu, Zhiyang]Fuzhou Univ, Coll Chem, State Key Lab Photocatalysis Energy & Environm, Fuzhou 350002, Peoples R China
  • [ 4 ] [Su, Xiaohui]Xiamen Univ, Coll Mat, Fujian Key Lab Adv Mat, Key Lab High Performance Ceram Fibers,Minist Educ, Xiamen 361005, Peoples R China
  • [ 5 ] [Li, Siwei]Xiamen Univ, Coll Mat, Fujian Key Lab Adv Mat, Key Lab High Performance Ceram Fibers,Minist Educ, Xiamen 361005, Peoples R China
  • [ 6 ] [Gu, Hui]Shanghai Univ, Sch Mat Sci & Engn, Mat Genome Inst, Shanghai 200444, Peoples R China
  • [ 7 ] [Luo, Jian]Univ Calif San Diego, Dept NanoEngn, Program Mat Sci & Engn, La Jolla, CA 92093 USA
  • [ 8 ] [Yin, Xiaowei]Northwestern Polytech Univ, Sci & Technol Thermostrucutral Composite Mat Lab, Xian 710072, Peoples R China
  • [ 9 ] [Yu, Zhiyang]Xiamen Tungsten Co LTD, Xiamen 361126, Fujian, Peoples R China

Reprint 's Address:

  • 喻志阳

    [Yu, Zhiyang]Fuzhou Univ, Coll Chem, State Key Lab Photocatalysis Energy & Environm, Fuzhou 350002, Peoples R China

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Source :

CERAMICS INTERNATIONAL

ISSN: 0272-8842

Year: 2020

Issue: 8

Volume: 46

Page: 10279-10283

4 . 5 2 7

JCR@2020

5 . 1 0 0

JCR@2023

ESI Discipline: MATERIALS SCIENCE;

ESI HC Threshold:196

JCR Journal Grade:1

CAS Journal Grade:1

Cited Count:

WoS CC Cited Count: 8

SCOPUS Cited Count: 10

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 4

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