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This paper aims to improve the magnetic properties of sintered Nd-Fe-B magnet. Ni powders were added to the Nd-Fe-B magnet through intergranular addition, and their effects on the microstructure and magnetic properties of the magnet were investigated. By adding a proper amount of Ni (0.3 wt%), the intrinsic coercivity H-cj of Nd-Fe-B magnet is significantly improved with only a slight decrease in the remanence B-r and the maximum energy product (BH)(max). The microstructural and compositional analyses reveal that Ni atoms not only enter the matrix phase but also concentrate in the intergranular regions either as Ni-containing Nd-rich phase or as Ni particles. This is consistent with the thermodynamic calculation results. Furthermore, a sintering mechanism of magnet with intergranular addition of Ni powders is tentatively proposed. These results may provide a reference for improving the magnetic properties of sintered Nd-Fe-B magnets. (C) 2017 Published by Elsevier B.V.
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JOURNAL OF ALLOYS AND COMPOUNDS
ISSN: 0925-8388
Year: 2017
Volume: 726
Page: 846-851
3 . 7 7 9
JCR@2017
5 . 8 0 0
JCR@2023
ESI Discipline: MATERIALS SCIENCE;
ESI HC Threshold:306
JCR Journal Grade:1
CAS Journal Grade:1
Cited Count:
WoS CC Cited Count: 19
SCOPUS Cited Count: 22
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 0
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