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Abstract:
A simple two-step/one-pot and highly efficient strategy for the synthesis of negletein from naturally abundant and inexpensive baicalin has been developed. In this one-pot sequence, esterification of baicalin catalyzed by concentrated H2SO4 in methanol followed by the treatment with excess NaBH4 afforded negletein in moderate yield. This method provides an additional approach for the synthesis of negletein. (C) 2016 Elsevier Ltd. All rights reserved.
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TETRAHEDRON LETTERS
ISSN: 0040-4039
Year: 2016
Issue: 18
Volume: 57
Page: 2001-2005
2 . 1 9 3
JCR@2016
1 . 5 0 0
JCR@2023
ESI Discipline: CHEMISTRY;
ESI HC Threshold:235
JCR Journal Grade:2
CAS Journal Grade:3
Cited Count:
WoS CC Cited Count: 4
SCOPUS Cited Count: 4
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
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30 Days PV: 0
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