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author:

Dai, P.-Q. (Dai, P.-Q..) [1] | Yu, H. (Yu, H..) [2] | Li, Q. (Li, Q..) [3]

Indexed by:

Scopus PKU CSCD

Abstract:

Nanocrystalline nickel was synthesized by direct current electrodeposition from a modified Watts-type bath. X-ray diffraction and transmission electron microscopy were used to characterize the microstructure of nickel deposits. The results show that nanocrytalline nickel with grain sizes in the range of 20-50 nm can be synthesized from saccharin-containing Watts-type baths with the current density range of 5-30 A/dm2. There existed preferred orientation in the deposits and it changed progressively from a (200) fibre texture to a (111) (200) double fibre texture as saccharin concentration increased. The hardness of the deposits increased prominently as grain size decreased to nanometer range.

Keyword:

Electrodeposition; Nanocrystalline; Nickel

Community:

  • [ 1 ] [Dai, P.-Q.]Coll. of Mat. Sci. and Eng., Fuzhou Univ., Fuzhou, China
  • [ 2 ] [Yu, H.]Coll. of Mat. Sci. and Eng., Fuzhou Univ., Fuzhou, China
  • [ 3 ] [Li, Q.]Coll. of Mat. Sci. and Eng., Fuzhou Univ., Fuzhou, China

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Source :

Transactions of Materials and Heat Treatment

ISSN: 1009-6264

Year: 2004

Issue: 5

Volume: 25

Page: 1283-1286

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 1

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