Characterizations of some N-substituted-salicylhydrazide in mixtures by NMR diffusion ordered spectroscopy - Details

author：

Zhang, F. (Zhang, F..) ^[1] | Yu, X.-Y. (Yu, X.-Y..) ^[2] | Chen, Z. (Chen, Z..) ^[3] | Lin, S. (Lin, S..) ^[4] | Liu, S.-X. (Liu, S.-X..) ^[5]

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Abstract：

Several　novel　N-substituted-salicylhydrazide　ligands,　most　of　which　are　difficult　to　be　purified　or　recrystallized　so　that　their　chemical　configurations　can　not　be　confirmed　by　conventional　NMR　and/or　X-ray　diffraction　techniques,　were　synthesized　in　this　experiment,　and　their　chemical　configurations　in　mixture　were　analyzed　and　characterized　by　2D　NMR　diffusion　ordered　spectroscopy　(DOSY),　a　labor-saving　virtual　separation　based　on　diffusion　properties,　together　with　several　routine　NMR　techniques.

Keyword：

Configuration; DOSY; N-substituted-salicylhydrazide; NMR; Synthesis

Community：

[ 1 ] [Zhang, F.]Department of Chemistry and Physics, Stt. Key Lab. Phys. Chem. Solid S., Xiamen University, Xiamen 361005, China
[ 2 ] [Zhang, F.]Stt. Key Lab. of Struct. Chemistry, Fuzhou 350002, China
[ 3 ] [Yu, X.-Y.]Department of Chemistry and Physics, Stt. Key Lab. Phys. Chem. Solid S., Xiamen University, Xiamen 361005, China
[ 4 ] [Yu, X.-Y.]Stt. Key Lab. of Struct. Chemistry, Fuzhou 350002, China
[ 5 ] [Chen, Z.]Department of Chemistry and Physics, Stt. Key Lab. Phys. Chem. Solid S., Xiamen University, Xiamen 361005, China
[ 6 ] [Chen, Z.]Stt. Key Lab. of Struct. Chemistry, Fuzhou 350002, China
[ 7 ] [Lin, S.]Department of Chemistry, Fuzhou University, Fuzhou 350002, China
[ 8 ] [Lin, S.]Stt. Key Lab. of Struct. Chemistry, Fuzhou 350002, China
[ 9 ] [Lin, S.]Department of Chemistry, Fujian Normal University, Fuzhou 350002, China
[ 10 ] [Liu, S.-X.]Department of Chemistry, Fuzhou University, Fuzhou 350002, China
[ 11 ] [Liu, S.-X.]Stt. Key Lab. of Struct. Chemistry, Fuzhou 350002, China

Reprint 's Address：

[Chen, Z.]Department of Chemistry and Physics, Stt. Key Lab. Phys. Chem. Solid S., Xiamen University, Xiamen 361005, China

Email：

chenz@jingxian.xmu.edu.cn

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Source ：

CHINESE JOURNAL OF STRUCTURAL CHEMISTRY

ISSN： 0254-5861

CN： 35-1112/TQ

Year： 2003

Issue： 3

Volume： 22

Page： 287-292

0 . 5 4 8

JCR@2003

5 . 9 0 0

JCR@2023

JCR Journal Grade：3

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ESI Highly Cited Papers on the List： 0 Unfold All

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