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Abstract:
The title compound C9H11N3O2 has been synthesized. The crystal belongs to the monoclinic system, space group C2/c with cell parameters: a=13.703(1), b=9.142(1), c=16.437(2) Å, β =105.547(3)°, V=1983.8(4)Å3, Z=8, Dc=1.294g/cm3, Mr=193.21, F(000)= 816, μ(MoKα)=0.094 mm-1. Final R and wR are 0.0527 and 0.1517, respectively, for 1596 [I≥2σ(I)] observed reflections. There are intermolecular hydrogen bonds in the crystal. The network structure was formed through the intermolecular hydrogen bonds. The hydrogen bond lengths of N(2)-H⋯N (1a)(a: -x+1, y, -z+1/2) and N(3)-H⋯O(2b)(b: -x+1/2, y-1/2, -z+1/2) are 3.007(2) and 2.786(2)Å, respectively.
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CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
ISSN: 0254-5861
CN: 35-1112/TQ
Year: 2001
Issue: 3
Volume: 20
Page: 227-228
0 . 1 8 4
JCR@2001
5 . 9 0 0
JCR@2023
JCR Journal Grade:4
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 2
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