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author:

Wu, W.-S. (Wu, W.-S..) [1] | Liu, S.-X. (Liu, S.-X..) [2]

Indexed by:

Scopus PKU CSCD

Abstract:

The title compound C9H11N3O2 has been synthesized. The crystal belongs to the monoclinic system, space group C2/c with cell parameters: a=13.703(1), b=9.142(1), c=16.437(2) Å, β =105.547(3)°, V=1983.8(4)Å3, Z=8, Dc=1.294g/cm3, Mr=193.21, F(000)= 816, μ(MoKα)=0.094 mm-1. Final R and wR are 0.0527 and 0.1517, respectively, for 1596 [I≥2σ(I)] observed reflections. There are intermolecular hydrogen bonds in the crystal. The network structure was formed through the intermolecular hydrogen bonds. The hydrogen bond lengths of N(2)-H⋯N (1a)(a: -x+1, y, -z+1/2) and N(3)-H⋯O(2b)(b: -x+1/2, y-1/2, -z+1/2) are 3.007(2) and 2.786(2)Å, respectively.

Keyword:

Crystal structure; Dihydrazide; Synthesis

Community:

  • [ 1 ] [Wu, W.-S.]Central Laboratory, Fuzhou University, Fuzhou 350002, China
  • [ 2 ] [Wu, W.-S.]College of Material, Huaqiao University, Quanzhou 362011, China
  • [ 3 ] [Liu, S.-X.]Central Laboratory, Fuzhou University, Fuzhou 350002, China

Reprint 's Address:

  • [Liu, S.-X.]Central Laboratory, Fuzhou University, Fuzhou 350002, China

Email:

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Source :

CHINESE JOURNAL OF STRUCTURAL CHEMISTRY

ISSN: 0254-5861

CN: 35-1112/TQ

Year: 2001

Issue: 3

Volume: 20

Page: 227-228

0 . 1 8 4

JCR@2001

5 . 9 0 0

JCR@2023

JCR Journal Grade:4

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

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