Synthesis, Crystal Structure, and Spectroscopic Properties of 5-Ethoxycarbonyl-4-[(4-methoxy-carbonyl)phenyl] -6-methyl-3,4-dihydropyrimidin2(1H)-ones - Details

author：

Peng, H.-N. (Peng, H.-N..) ^[1] | Zheng, D.-G. (Zheng, D.-G..) ^[2] | Zeng, X.-H. (Zeng, X.-H..) ^[3] | Hu, J.-R. (Hu, J.-R..) ^[4] | Ye, H.-D. (Ye, H.-D..) ^[5]

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Abstract：

The　title　compound,　5-ethoxycarbonyl-4-[(4-methoxycarbonyl)phenyl]-6-methyl-3,4-dihydropyrimidin-2(1H)-ones　(1),　was　synthesized　from　the　one-pot,　three-component　condensation　reactions　and　characterized　by　FTIR,　1H　NMR,　HRMS,　and　single　crystal　X-ray　diffraction.　The　compound　(1)　crystallizes　in　a　triclinic　system,　space　group　P-1　with　a　=　6.1874(12),　b　=　7.5715(15),　c　=　17.369(4)Å,　=　80.24(3),　β　=　81.15(3),　γ　=　76.93(3)○,　and　Z　=　2.　The　molecules　are　linked　by　hydrogen　bonds　N-H···O　and　C-H···O　to　generate　a　2D　network.　In　addition,　UV-visible　and　fluorescence　spectral　measurements　prove　that　it　shows　positive　solvatochromic　effect　as　the　solvent　polarity　was　increased.　Copyright　©　Taylor　&　Francis　Group,　LLC.

Keyword：

3,4-dihydropyrimidin-2(1H)-ones; Crystal structure; fluorescence; solvatochromic effect; synthesis

Community：

[ 1 ] [Peng, H.-N.]Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi, Province, Shangrao Normal University, Shangrao, China
[ 2 ] [Zheng, D.-G.]Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi, Province, Shangrao Normal University, Shangrao, China
[ 3 ] [Zeng, X.-H.]College of Chemistry and Chemical Engineering, Fuzhou University, Fuzhou, FuJian, China
[ 4 ] [Hu, J.-R.]Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi, Province, Shangrao Normal University, Shangrao, China
[ 5 ] [Ye, H.-D.]Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi, Province, Shangrao Normal University, Shangrao, China

Reprint 's Address：

[Peng, H.-N.]Key Laboratory of Applied Organic Chemistry, Higher Institutions of Jiangxi, Province, Shangrao Normal UniversityChina

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Source ：

Molecular Crystals and Liquid Crystals

ISSN： 1542-1406

Year： 2015

Issue： 1

Volume： 609

Page： 266-276

0 . 5 3 2

JCR@2015

0 . 7 0 0

JCR@2023

ESI HC Threshold：265

JCR Journal Grade：4

CAS Journal Grade：4

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SCOPUS Cited Count： 1

ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 1

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