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author:

Yang, Y. (Yang, Y..) [1] | Lin, X. (Lin, X..) [2] | Zheng, Z. (Zheng, Z..) [3] | Lin, G. (Lin, G..) [4] | Zhang, Y. (Zhang, Y..) [5] | You, Y. (You, Y..) [6] | Weng, Z. (Weng, Z..) [7]

Indexed by:

Scopus

Abstract:

Herein we disclose the report on the synthesis of α-trifluoromethylseleno-substituted ketone derivatives via copper-mediated trifluoromethylselenolation of α-bromoketones with [(bpy)Cu(SeCF3)]2 1. A broad range of substituted 2-bromoacetophenone substrates were found to react smoothly with 1 in the presence of 3 equiv of K3PO4 to afford the corresponding α-trifluoromethylseleno-substituted ketones in good yields. A wide range of functional groups were well tolerated and the reaction conditions are amenable to scale up. © 2017 Elsevier B.V.

Keyword:

Copper; Fluorine; Trifluoromethylselenolation; α-Bromoketones

Community:

  • [ 1 ] [Yang, Y.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China
  • [ 2 ] [Lin, X.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China
  • [ 3 ] [Zheng, Z.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China
  • [ 4 ] [Lin, G.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China
  • [ 5 ] [Zhang, Y.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China
  • [ 6 ] [You, Y.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China
  • [ 7 ] [Weng, Z.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityFujian 350108, China

Reprint 's Address:

  • [You, Y.]State Key Laboratory of Photocatalysis on Energy and Environment, College of Chemistry, Fuzhou UniversityChina

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Source :

Journal of Fluorine Chemistry

ISSN: 0022-1139

Year: 2017

Volume: 204

Page: 1-5

1 . 8 7 9

JCR@2017

1 . 7 0 0

JCR@2023

ESI HC Threshold:226

JCR Journal Grade:2

CAS Journal Grade:3

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 17

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 1

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