Efficient synthesis of new asymmetric tripodal ligands using microwave irradiation, and their crystal structures - Details

author：

Yuan, Z. (Yuan, Z..) ^[1] | Yang, X. (Yang, X..) ^[2] | Wang, L. (Wang, L..) ^[3] | Huang, J. (Huang, J..) ^[4] | Wei, G. (Wei, G..) ^[5]

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Abstract：

An　efficient　method　for　the　synthesis　of　asymmetric　tripodal　ligands　from　aryl　aldehydes　and　(2-hydro-xybenzyl-2-pyri-dylmethyl)amine　was　developed.　It　has　the　advantages　of　short　reaction　times,　high　yields　and　a　simple　methodology.　The　title　ligands　were　characterized　using　a　combination　of　1H　NMR,　13C　NMR,　FT-IR　and　H　RMS　spectroscopies.　The　structures　of　some　of　the　ligand　were　confirmed　by　single-crystal　X-ray　diffraction.　This　journal　is　©　the　Partner　Organisations　2014.

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[ 1 ] [Yuan, Z.]College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 2 ] [Yuan, Z.]School of Pharmacy, Zunyi Medical University, Zunyi, Guizhou, 563003, China
[ 3 ] [Yang, X.]College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 4 ] [Wang, L.]College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 5 ] [Huang, J.]College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 6 ] [Wei, G.]CSIRO Materials Science and Engineering, PO Box 218, Lindfield, NSW 2070, Australia

Reprint 's Address：

[Huang, J.]College of Chemistry, Fuzhou UniversityChina

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RSC Advances

ISSN： 2046-2069

Year： 2014

Issue： 79

Volume： 4

Page： 42211-42214

3 . 8 4

JCR@2014

3 . 9 0 0

JCR@2023

ESI HC Threshold：268

JCR Journal Grade：1

CAS Journal Grade：3

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SCOPUS Cited Count： 6

ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 0

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