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author:

Liu, J.R. (Liu, J.R..) [1] | Hong, R.Y. (Hong, R.Y..) [2] | Feng, W.G. (Feng, W.G..) [3] | Badami, D. (Badami, D..) [4] | Wang, Y.Q. (Wang, Y.Q..) [5]

Indexed by:

Scopus

Abstract:

Large-scale production of strontium hexaferrite (SrFe12O19) particles was successfully achieved by molten-salt-assisted coprecipitation. A mixture of sodium hydroxide and sodium carbonate was served as mixed precipitant to obtain ferrite precursors. The effects of the Fe3+/Sr2+ molar ratio, calcination temperature, calcination time, and molten-salt amount on the formation, morphology and magnetic properties of SrFe12O19 particles were investigated. The resultant particles were characterized by Fourier transform infrared spectroscopy, thermogravimetric analysis, X-ray diffraction, scanning electron microscopy, and vibrating sample magnetometer. Single-phase SrFe12O19 particles, with particle sizes of 0.8-1.2μm, were obtained from the precursor (with a Fe3+/Sr2+ molar ratio of 10) being calcined at 950°C for 2h using the mass ratio (NaCl to precursor) of 0.3. The saturation magnetization, remanent magnetization and coercivity were about 62emu/g, 37emu/g, and 4310Oe, respectively. A comparison of the products obtained at different preparation-scales was also done. The results showed that it was easier to control the particle morphology using molten salt synthesis and more economical on a large-scale production. © 2014 Elsevier B.V.

Keyword:

Large-scale production; Magnetic properties; Molten salt synthesis; Strontium ferrite

Community:

  • [ 1 ] [Liu, J.R.]School of Chemical Engineering, Fuzhou University, Fuzhou 350108, China
  • [ 2 ] [Hong, R.Y.]School of Chemical Engineering, Fuzhou University, Fuzhou 350108, China
  • [ 3 ] [Hong, R.Y.]College of Chemistry, Chemical Engineering and Materials Science, Key Laboratory of Organic Synthesis of Jiangsu Province, Soochow University, Suzhou 215123, China
  • [ 4 ] [Feng, W.G.]Suzhou Nanocomp Inc., Suzhou New District, Suzhou 215011, China
  • [ 5 ] [Badami, D.]Department of Chemical Engineering, University of Waterloo, Ontario, N2L3G1, Canada
  • [ 6 ] [Wang, Y.Q.]College of Chemistry and Chemical Engineering, Yangzhou University, Yangzhou 225002, China

Reprint 's Address:

  • [Hong, R.Y.]School of Chemical Engineering, Fuzhou University, Fuzhou 350108, China

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Source :

Powder Technology

ISSN: 0032-5910

Year: 2014

Volume: 262

Page: 142-149

2 . 3 4 9

JCR@2014

4 . 5 0 0

JCR@2023

ESI HC Threshold:268

JCR Journal Grade:2

CAS Journal Grade:2

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 1

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