• Complex
  • Title
  • Keyword
  • Abstract
  • Scholars
  • Journal
  • ISSN
  • Conference
成果搜索

author:

Zhao, Y. (Zhao, Y..) [1] | Zheng, J. (Zheng, J..) [2] | Yang, M. (Yang, M..) [3] | Fu, F. (Fu, F..) [4] (Scholars:付凤富)

Indexed by:

Scopus PKU CSCD

Abstract:

A method for the detection of trace As (III), As (V), monomethylarsonic acid (MMA), dimethylarsinic acid (DMA), arsenocholine (AsC) and arsenobetaine (AsB) in seaweeds by capillary electrophoresis-inductively coupled plasma mass spectrometry (CE-ICP-MS) was developed. The optimized conditions of CE including chemical component; pH and concentration of the buffer; separation voltage and injection time were studied in detail. The results showed that the above six species of arsenic were baseline separated within 25 min under the optimized conditions. The relative standard deviations (n =6) of the peak areas were smaller than 5%, and the detection limits (calculated as As) (S/N = 3) were 0. 08 - 0. 12 μg/L for all the above six species of arsenic. The method has been successfully applied to the determination of the species of arsenic in kelp samples. The recoveries were 90% - 103%. The method has good reproducibility, high sensitivity; short analytical time and strong resistance to complex matrix, and can be used for the speciation analysis of arsenic in real seafood samples.

Keyword:

Arsenic; Capillary electrophoresis (CE); Inductively coupled plasma mass spectrometry (iCP-MS); Seaweeds; Speciation analysis

Community:

  • [ 1 ] [Zhao, Y.]Key Laboratory of Analysis and Detection for Food Safety of Ministry of Education, Fuzhou University, Fuzhou 350108, China
  • [ 2 ] [Zheng, J.]Key Laboratory of Analysis and Detection for Food Safety of Ministry of Education, Fuzhou University, Fuzhou 350108, China
  • [ 3 ] [Yang, M.]Key Laboratory of Analysis and Detection for Food Safety of Ministry of Education, Fuzhou University, Fuzhou 350108, China
  • [ 4 ] [Fu, F.]Key Laboratory of Analysis and Detection for Food Safety of Ministry of Education, Fuzhou University, Fuzhou 350108, China

Reprint 's Address:

  • 付凤富

    [Fu, F.]Key Laboratory of Analysis and Detection for Food Safety of Ministry of Education, Fuzhou University, Fuzhou 350108, China

Show more details

Related Keywords:

Related Article:

Source :

Chinese Journal of Chromatography (Se Pu)

ISSN: 1000-8713

Year: 2011

Issue: 2

Volume: 29

Page: 111-114

1 . 2 0 0

JCR@2023

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count: 11

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

Affiliated Colleges:

Online/Total:595/10927111
Address:FZU Library(No.2 Xuyuan Road, Fuzhou, Fujian, PRC Post Code:350116) Contact Us:0591-22865326
Copyright:FZU Library Technical Support:Beijing Aegean Software Co., Ltd. 闽ICP备05005463号-1