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author:

Li, X.-H. (Li, X.-H..) [1] | Yang, F. (Yang, F..) [2] | Lin, Z.-Y. (Lin, Z.-Y..) [3] | Qiu, B. (Qiu, B..) [4] | Wang, D.-H. (Wang, D.-H..) [5]

Indexed by:

Scopus PKU CSCD

Abstract:

Based on the initial near-infrared spectrum of edible essence samples and its mixture with DEHP and DINP, we chose the wavelength ranges of 8800~8540 and 7500~5085 cm-1 to use the principal component analysis (PCA) method to distinguish these three types of samples. The correct rate of the identification is proved to be 100%. Meanwhile, we measured the content of DEHP and DINP (with the concentration ranging between 0 and 100 mg·kg-1) in the edible essence and established the quantitative analysis model by using partial least squares (PLS). It was found that the relative errors of the prediction results of DEHP and DINP are -1.23%~3% and -1%~3.6%, respectively, and the relative root-mean-square errors of prediction (RRMSEP) of them are 1.39 and 0.98, respectively. This study provides a simple, rapid and accurate method to detect the additive dosage of plasticizing agents in edible essence in the food industry.

Keyword:

Cluster analysis (CA); Near-infrared spectrum (NIRS); Partial least-squares (PLS); Plasticizer; Principal component analysis (PCA)

Community:

  • [ 1 ] [Li, X.-H.]Fujian Provincial Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350108, China
  • [ 2 ] [Yang, F.]Fujian Entry-Exit Inspection and Quarantine Bureau of P.R.C, Fuzhou 350001, China
  • [ 3 ] [Lin, Z.-Y.]Fujian Provincial Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350108, China
  • [ 4 ] [Qiu, B.]Fujian Provincial Key Laboratory of Analysis and Detection Technology for Food Safety, Department of Chemistry, Fuzhou University, Fuzhou 350108, China
  • [ 5 ] [Wang, D.-H.]Fujian Entry-Exit Inspection and Quarantine Bureau of P.R.C, Fuzhou 350001, China

Reprint 's Address:

  • [Yang, F.]Fujian Entry-Exit Inspection and Quarantine Bureau of P.R.C, Fuzhou 350001, China

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Source :

Spectroscopy and Spectral Analysis

ISSN: 1000-0593

Year: 2013

Issue: 3

Volume: 33

Page: 690-693

0 . 2 7

JCR@2013

0 . 7 0 0

JCR@2023

JCR Journal Grade:4

CAS Journal Grade:4

Cited Count:

WoS CC Cited Count: 0

SCOPUS Cited Count: 2

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 3

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