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author:

Zheng, Y. (Zheng, Y..) [1] | Wang, R. (Wang, R..) [3] | Wei, K. (Wei, K..) [4]

Indexed by:

Scopus

Abstract:

In this study, we combined the traditional vacuum furnace with a sur-high accuracy vacuum gauge for measuring the change of gas pressure in the furnace as a function of temperature. The modified vacuum furnace was used for preparing silicon carbide (SiC), and the recorded data named thermobarogram were applied to detect the reaction temperature for synthesis of SiC, which, in particular, changes as catalysts are used. The results showed that the carbothermal reduction temperature for synthesizing SiC, under dynamic vacuum condition, would decrease to 850 °C when the mole ratio of Fe/Si=0.06 was employed in the SiC precursor. © 2007 Elsevier Ltd. All rights reserved.

Keyword:

Carbothermal reduction; Silicon carbide; Synthesis; Vacuum furnace

Community:

  • [ 1 ] [Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China
  • [ 2 ] [Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China
  • [ 3 ] [Wang, R.]National Engineering Research Center of Chemical Fertilizer Catalyst, Fuzhou University, Fuzhou, 350002, China
  • [ 4 ] [Wei, K.]National Engineering Research Center of Chemical Fertilizer Catalyst, Fuzhou University, Fuzhou, 350002, China

Reprint 's Address:

  • [Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China

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Source :

Vacuum

ISSN: 0042-207X

Year: 2007

Issue: 3

Volume: 82

Page: 336-339

0 . 8 8 1

JCR@2007

3 . 8 0 0

JCR@2023

JCR Journal Grade:3

Cited Count:

WoS CC Cited Count:

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 0

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