Synthesis of a novel mesoporous silicon carbide with a thorn-ball-like shape - Details

author：

Zheng, Y. (Zheng, Y..) ^[1] | Lin, L.-X. (Lin, L.-X..) ^[3] | Ni, J. (Ni, J..) ^[4] | Wei, K.-M. (Wei, K.-M..) ^[5]

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Abstract：

A　novel　kind　of　mesoporous　silicon　carbide　(SiC)　was　synthesized　via　the　carbothermal　reduction　reaction　of　carbonaceous　silicon　xerogel.　The　purified　SiC　sample　was　characterized　by　X-ray　diffraction,　Fourier　transform　infra-red　spectroscopy,　electron　microscopy　and　N2　porosimetry.　The　results　show　that　the　SiC　obtained　has　a　thorn-ball-like　(TBL)　shape.　The　TBL　SiC　sample　has　a　surface　area　of　141　m2/g　and　a　pore　diameter　in　the　range　of　2-30　nm,　and　possesses　two　different　kinds　of　pores.　©　2006　Acta　Materialia　Inc.

Keyword：

Carbothermal reduction; Mesoporous; Silicon carbide; Sol-gel

Community：

[ 1 ] [Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China
[ 2 ] [Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China
[ 3 ] [Lin, L.-X.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China
[ 4 ] [Ni, J.]National Engineering Research Center of Chemical Fertilizer Catalyst, Fuzhou University, Fuzhou, 350002, China
[ 5 ] [Wei, K.-M.]National Engineering Research Center of Chemical Fertilizer Catalyst, Fuzhou University, Fuzhou, 350002, China

Reprint 's Address：

[Zheng, Y.]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou, Fujian 350007, China

Email：

zhn63201@163.com

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Source ：

Scripta Materialia

ISSN： 1359-6462

Year： 2006

Issue： 10

Volume： 55

Page： 883-886

2 . 1 6 1

JCR@2006

5 . 3 0 0

JCR@2023

JCR Journal Grade：1

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