Electrochemical Continuous-Flow Scholl Reaction toward Polycyclic Aromatic Hydrocarbons - Details

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The　preparation　of　polycyclic　aromatic　hydrocarbons　(PAHs)　by　the　Scholl　reaction　is　typically　performed　by　using　superstoichiometric　oxidants.　Herein,　we　develop　an　electrochemical　continuous-flow　Scholl　reaction　to　access　PAHs　that　features　a　reduction　in　the　use　of　supporting　electrolytes　and　easy　scale-up　without　changing　the　reaction　conditions　and　setups.　This　reaction　allows　the　synthesis　of　distorted　PAHs　containing　three　[5]helicene　units　that　possess　intriguing　electronic　and　optical　properties.　©　2024　American　Chemical　Society.

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[ 1 ] [Wang W.-Z.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 2 ] [Wang Q.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 3 ] [He X.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 4 ] [Shen Y.-H.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 5 ] [Zhai Z.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 6 ] [Zhang R.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 7 ] [Li Y.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China
[ 8 ] [Ye K.-Y.]Key Laboratory of Molecule Synthesis and Function Discovery, Fujian Province University, College of Chemistry, Fuzhou University, Fuzhou, 350108, China

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Organic Letters

ISSN： 1523-7060

Year： 2024

Issue： 11

Volume： 26

Page： 2243-2248

4 . 9 0 0

JCR@2023

CAS Journal Grade：1

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ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 1

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