FSO 2 Radical-Initiated Photoredox Cyclization of 4-Enoic Acids to Functionalized γ-Lactones - Details

author：

Fang, Xin (Fang, Xin.) ^[1] | Geng, Xuebing (Geng, Xuebing.) ^[2] | Wang, Peng (Wang, Peng.) ^[3] | Zhang, Honghai (Zhang, Honghai.) ^[4] | Liao, Saihu (Liao, Saihu.) ^[5]

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Abstract：

The　incorporation　of　sulfonyl　fluoride　groups　into　molecules　has　been　proven　effective　in　enhancing　their　biological　activities　or　introducing　new　functions.　Herein,　a　transition-metal-free　and　visible-　light-mediated　radical　tandem　cyclization　of　unsaturated　carboxylic　acid　is　reported.　This　affords　a　facile　access　to　FSO2-functionalized　lactones　efficiently,　which　are　critical　structural　motifs　widely　present　in　biologically　active　molecules.　©　2024　Georg　Thieme　Verlag.　All　rights　reserved.

Keyword：

Cyclization Esters Fluorine compounds Molecules Transition metals

Community：

[ 1 ] [Fang, Xin]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou; 350116, China
[ 2 ] [Geng, Xuebing]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou; 350116, China
[ 3 ] [Wang, Peng]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou; 350116, China
[ 4 ] [Wang, Peng]Key Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, Huaibei Normal University, Huaibei, Anhui; 235000, China
[ 5 ] [Zhang, Honghai]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou; 350116, China
[ 6 ] [Zhang, Honghai]State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen; 361005, China
[ 7 ] [Liao, Saihu]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou; 350116, China
[ 8 ] [Liao, Saihu]State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen; 361005, China

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Source ：

Synthesis (Germany)

ISSN： 0039-7881

Year： 2024

Issue： 11

Volume： 56

Page： 1727-1734

2 . 2 0 0

JCR@2023

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SCOPUS Cited Count： 3

ESI Highly Cited Papers on the List： 0 Unfold All

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