Synthesis of FSO2-Functionalized Oxindoles via a Radical Fluorosulfonylation/Intramolecular Arylation Cascade - Details

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Herein,　we　report　the　development　of　a　FSO2　radical　initiated　tandem　cyclization　reaction　under　visible　light　photoredox　catalysis,　which　allows　for　a　facile　access　to　FSO2-functionalized　oxindoles　from　Narylacrylamides.　This　reaction　features　mild　reaction　conditions,　readily　available　starting　materials,　and　SuFExable　products.　The　introduction　of　sulfonyl　fluoride　groups　into　oxindoles　could　be　of　interest　for　related　study　in　the　context　of　discovering　new　bioactive　molecules.　©　2024.　Thieme.　All　rights　reserved.

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click chemistry FSO2 radicals oxindoles photoredox catalysis SuFEx

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[ 1 ] [Yang N.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 2 ] [Pei G.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 3 ] [Li H.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 4 ] [Han J.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 5 ] [Wang P.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 6 ] [Wang P.]Key Laboratory of Green and Precise Synthetic Chemistry and Applications, Ministry of Education, Huaibei Normal University, Anhui, Huaibei, 235000, China
[ 7 ] [Xie L.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 8 ] [Liao S.]Key Laboratory of Molecule Synthesis and Function Discovery, College of Chemistry, Fuzhou University, 2 Xueyuan Road, Fuzhou, 350116, China
[ 9 ] [Liao S.]State Key Laboratory of Physical Chemistry of Solid Surfaces, Xiamen University, Xiamen, 361005, China

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Synthesis (Germany)

ISSN： 0039-7881

Year： 2024

2 . 2 0 0

JCR@2023

CAS Journal Grade：4

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ESI Highly Cited Papers on the List： 0 Unfold All

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30 Days PV： 3

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