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author:

Li, Yang (Li, Yang.) [1] | Lv, Pengcheng (Lv, Pengcheng.) [2] | Ye, Wenchao (Ye, Wenchao.) [3] | Zhou, Jun (Zhou, Jun.) [4] | Chen, Yu (Chen, Yu.) [5] | Li, Kun (Li, Kun.) [6] | Wu, Chaochao (Wu, Chaochao.) [7] | Liang, Xiaoyu (Liang, Xiaoyu.) [8] | Lin, Feng (Lin, Feng.) [9]

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EI

Abstract:

Non-weldable nickel-based superalloys fabricated via electron beam powder bed fusion exhibit pronounced preferential grain growth orientation, resulting in significant anisotropic mechanical behavior. This study demonstrates a methodology for controlling anisotropic microstructures in Inconel 939 through process parameter optimization, specifically by modulating EB-PBF energy density to tailor mechanical properties. Electron backscatter diffraction analysis revealed distinct microstructural characteristics: the lowest energy density sample (E1) displayed elongated columnar grains with strong texture (aspect ratio ∼15.86), while the highest energy density sample (E3) contained uniformly oriented near-equiaxed grains (aspect ratio ∼3.94). Transmission electron microscopy characterization of tensile specimens indicated that along the parallel building direction, E1 exhibited extensive dislocation pile-ups and bypass mechanisms. With increasing energy density, E2 demonstrated enhanced dislocation accumulation with partial shearing at carbide peripheries, whereas E3 showed complete dislocation penetration through entire carbide strengthening phases. Tensile testing quantified the anisotropic ultimate tensile strength differentials: 348.7 MPa for E1, 130.4 MPa for E2, and 47.6 MPa for E3. Regarding anisotropic yield strength differences, E2 exhibited significantly reduced yield strength due to carbide coarsening, resulting in larger anisotropy differentials compared to both E1 and E3 samples. Nevertheless, E1 and E3 still followed the trend of progressively reduced anisotropy. The results establish that strategic energy density control enables microstructural isotropization through combined grain morphology modification and optimization of dislocation-mediated strengthening mechanisms. © 2025 Elsevier B.V.

Keyword:

Anisotropy Aspect ratio Carbides Coarsening Density (specific gravity) Electron beams Electrons Grain growth Nickel alloys Strengthening (metal) Superalloys Tensile strength Tensile testing Textures Transmission electron microscopy Yield stress

Community:

  • [ 1 ] [Li, Yang]Department of Mechanical Engineering, Tsinghua University, Beijing; 100084, China
  • [ 2 ] [Lv, Pengcheng]Institute of Laser Intelligent Manufacturing and Precision Processing, School of Mechanical Engineering, Guangxi University, Guangxi, Nanning; 530004, China
  • [ 3 ] [Ye, Wenchao]School of Mechanical Engineering and Automation, Fuzhou University, Fuzhou; 350108, China
  • [ 4 ] [Zhou, Jun]Institute of Laser Intelligent Manufacturing and Precision Processing, School of Mechanical Engineering, Guangxi University, Guangxi, Nanning; 530004, China
  • [ 5 ] [Chen, Yu]School of Mechanical Engineering, Chengdu University, Chengdu; 610106, China
  • [ 6 ] [Li, Kun]State Key Laboratory of Mechanical Transmission for Advanced Equipment, Chongqing University, Chongqing; 400044, China
  • [ 7 ] [Wu, Chaochao]School of Mechanical Engineering and Automation, Fuzhou University, Fuzhou; 350108, China
  • [ 8 ] [Liang, Xiaoyu]Department of Mechanical Engineering, Tsinghua University, Beijing; 100084, China
  • [ 9 ] [Lin, Feng]Department of Mechanical Engineering, Tsinghua University, Beijing; 100084, China

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Source :

Journal of Alloys and Compounds

ISSN: 0925-8388

Year: 2025

Volume: 1041

5 . 8 0 0

JCR@2023

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ESI Highly Cited Papers on the List: 0 Unfold All

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Chinese Cited Count:

30 Days PV: 0

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