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学者姓名：李宝铭
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Abstract ：
稀土上转换纳米粒子(UCNPs)因其具有毒性小、化学稳定性好和背景荧光低等优点被用于构建荧光纳米传感器.通过溶剂热法制备核壳UCNPs,采用柠檬酸钠对其进行表面配体交换得到水溶性核壳UCNPs(Cit-CS-UCNPs),以Cit-CS-UCNPs作为荧光传感器的能量供体,二氧化锰(MnO2)纳米片作为荧光传感器的能量受体,采用荧光共振能量转移(FRET)机理,构建了一种用于食品添加剂二氧化氢(H2O2)和叔丁基对苯二酚(TBHQ)检测的荧光纳米传感器(Cit-CS-UCNPs-MnO2).通过扫描电镜(SEM)、荧光光谱和紫外可见吸收光谱(UV-Vis)等分析测试手段对制备的纳米材料的形貌结构和性能进行表征.考察了猝灭剂浓度、孵育温度及孵育时间等实验条件对荧光传感体系检测性能的影响.荧光光谱和UV-Vis实验结果表明,Cit-CS-UCNPs最大发射峰位于654 nm,Cit-CS-UCNPs与MnO2结合后,核壳UCNPs发生荧光猝灭,当存在H2O2时,Cit-CS-UCNPs的荧光恢复,说明在此波段H2O2与MnO2纳米片发生氧化还原反应,MnO2纳米片被还原成Mn2+,逐渐从Cit-CS-UCNPs的表面解离下来;存在TBHQ时,Cit-CS-UCNPs-MnO2与TBHQ体系峰位与TBHQ偏移到253 nm,为TBHQ与MnO2纳米片发生氧化还原反应,使得Cit-CS-UCNPs-MnO2体系中FRET效应减弱,荧光强度回升.SEM结果表明,MnO2纳米片均匀包覆在Cit-CS-UCNPs的周围,在水中仍可保持良好的分散性,表明MnO2纳米片修饰到Cit-CS-UCNPs表面.对猝灭剂高锰酸钾(KMnO4)的浓度进行了优化.结果表明,当KMnO4浓度为10 mol·L-1时,猝灭效率可达90％.对检测条件进行优化,结果表明H2O2的检测孵育时间为25 min时,MnO2和H2O2之间氧化还原反应基本完全,Cit-CS-UCNPs-MnO2荧光恢复值最大;TBHQ的检测孵育时间为30 min.在最佳实验条件下,Cit-CS-UCNPs-MnO2 的荧光强度变化比率与 H2O2 浓度(0～1 000 μmol·L-1)及 TBHQ 浓度(0～0.6 mmol·L-1)分别具有良好的线性关系.保持最佳实验条件,选取食品中存在的代表性金属离子(如K+、Na+、Ca2+和Mg2+)和常见的食品添加剂苯甲酸(BA)、D-葡萄糖(Glu)、山梨酸钾(PS)、蔗糖(Suc)、纳他霉素(Nat)和肌醇(Ino)作为研究对象进行选择性测试,发现与H2O2相比,Cit-CS-UCNPs-MnO2对其他添加物质没有强烈的反应,传感器整体荧光信号波动不大,因此Cit-CS-UCNPs-MnO2对H2O2和TBHQ可进行特异性检测.
Keyword ：
上转换纳米粒子 上转换纳米粒子 核壳结构 核壳结构 荧光纳米传感器 荧光纳米传感器
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| GB/T 7714 | 张璇 , 王雅森 , 温娜 et al. 基于稀土上转换纳米粒子传感器的构建及其在食品添加剂检测中的应用 [J]. | 光谱学与光谱分析 , 2024 , 44 (9) : 2459-2466 . |
| MLA | 张璇 et al. "基于稀土上转换纳米粒子传感器的构建及其在食品添加剂检测中的应用" . | 光谱学与光谱分析 44 . 9 (2024) : 2459-2466 . |
| APA | 张璇 , 王雅森 , 温娜 , 吕海霞 , 李宝铭 . 基于稀土上转换纳米粒子传感器的构建及其在食品添加剂检测中的应用 . | 光谱学与光谱分析 , 2024 , 44 (9) , 2459-2466 . |
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Rare earth up-conversion nanoparticles (UCNPs) have been used to construct fluorescent nanosensors because of their low toxicity, good chemical stability, and low background fluorescence. Core-shell UCNPs were prepared using the solvothermal method, and water-soluble core-shell UCNPs (Cit-CS-UCNPs) were obtained by surface ligand exchange with sodium citrate. The Cit-CS-UCNPs were used as the energy donor of the fluorescence sensor, and manganese dioxide (MnO2) nanosheets were used as the energy receptor of the fluorescence sensor. Based on the fluorescence resonance energy transfer (FRET) mechanism, a fluorescence nanosensor (Cit-CS-UCNPs-MnO2) was constructed for the detection of hydrogen dioxide (H2O2) and tert-butylhydroquinone (TBHQ ) as food additives. The prepared nanomaterials' morphology, structure, and properties were characterized by scanning electron microscopy (SEM), fluorescence spectrum, and ultraviolet spectrum (UV-vis). The effects of quenching agent concentration, incubation temperature, and incubation time on the detection performance of the fluorescence sensing system were investigated. According to the fluorescence spectra and UV-Vis experimental results, the maximum emission peak of Cit-CS-UCNPs is 654 nm. After the combination of Cit-CS-UCNPs and MnO2, core-shell UCNPs undergo fluorescence quenching. When H2O2 is present, the fluorescence of Cit-CS-UCNPs recovers. The results indicate that H2O2 and MnO2 nanosheets undergo redox reaction at this band, and MnO2 nanosheets are reduced to Mn2+, which gradually dissociates from the surface of Cit-CS-UCNPs. In the presence of TBHQ, the peak of the Cit-CS-UCNPs-MnO2 and TBHQ system was shifted to 253 nm, indicating that the redox reaction occurred between TBHQ and MnO2 nanosheets, and the FRET effect was reduced in the Cit-CS-UCNPs-MnO2 system, and the fluorescence intensity increased. It can be seen from the SEM results that MnO2 nanosheets are uniformly coated around Cit-CS-UCNPs, and maintain good dispersion in water, indicating that MnO2 nanosheets are modified on the surface of Cit-CS-UCNPs. The concentration of the quencher potassium permanganate (KMnO4) was optimized, and the results showed that when the concentration of KMnO4 is 10 mol.L-1, the quenching efficiency can reach 90%. The detection conditions were optimized, and the results showed that when the incubation time of H2O2 was 25 min, the redox reaction between MnO2 and H2O2 was complete. The fluorescence recovery value of Cit-CS-UCNPs-MnO2 was the maximum. The incubation time of TBHQ was 30 min. Under the optimal experimental conditions, the fluorescence intensity of Cit-CS-UCNPs-MnO2 has a good linear relationship with the concentration of H2O2 (0 similar to 1 000 mu mol.L-1) and TBHQ (0 similar to 0.6 mmol.L-1). The optimal experimental conditions were maintained, and representative metal ions (such as K+, Na+, Ca2+ and Mg2+) and common food additives (BA, Glu, PS, Suc, Nat and Ino) in food were selected as research objects. The results showed that compared with H2O2, Cit-CS-UCNPs-MnO2 did not react strongly to other added substances, and the overall fluorescence signal of the sensor did not fluctuate much. Therefore, it can be seen that Cit-CS-UCNPs-MnO2 can detect the specificity of H2O2 and TBHQ.
Keyword ：
Core shell structures Core shell structures Fluorescent nanosensor Fluorescent nanosensor Up conversion nanoparticles Up conversion nanoparticles
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| GB/T 7714 | Zhang, Xuan , Wang, Ya-sen , Na, Wen et al. Construction of a Rare Earth Up-Conversion Nanoparticle Sensor and Its Application in the Detection of Food Additives [J]. | SPECTROSCOPY AND SPECTRAL ANALYSIS , 2024 , 44 (9) : 2459-2466 . |
| MLA | Zhang, Xuan et al. "Construction of a Rare Earth Up-Conversion Nanoparticle Sensor and Its Application in the Detection of Food Additives" . | SPECTROSCOPY AND SPECTRAL ANALYSIS 44 . 9 (2024) : 2459-2466 . |
| APA | Zhang, Xuan , Wang, Ya-sen , Na, Wen , Lu, Hai-xia , Li, Bao-ming . Construction of a Rare Earth Up-Conversion Nanoparticle Sensor and Its Application in the Detection of Food Additives . | SPECTROSCOPY AND SPECTRAL ANALYSIS , 2024 , 44 (9) , 2459-2466 . |
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Poly(lactic acid) (PLA) grafted glycidyl neodecanoate (GND) with a single epoxy group (PLA-GND) is prepared in this paper by solid phase grafting, and the effects of different reaction conditions on the grafting percentage of PLA-GND are investigated. Furthermore, PLA-GND is used as a nonreactive compatibilizer to prepare PLA-GND/PLA/poly(butylene adipate-co-terephthalate) (PBAT) composite by melt blending. The results show that PLA-GND has the highest grafting percentage of 2.15% when the feed weight ratio of GND to PLA is 0.2, the feed weight ratio of triphenylphosphine to PLA is 0.02, the additive amount of xylene is 1 mL, the reaction temperature is 120 degrees C, and the reaction time is 115 min. The GND segments of PLA-GND and PBAT segments could form a physical entanglement microdomain because of the similar aliphatic chain of GND and PBAT, which would improve the compatibility of PLA and PBAT. PLA-GND/PLA/PBAT composite has the highest tensile strength, elongation at break, impact strength, crystallinity, heat deformation temperature, and melt flow rate at a PLA-GND content of 5%, which are 38.54 MPa, 118.65%, 15.83 kJ/m2, 5.71%, 65.3 degrees C, and 36.3 g/10 min, 14.53%, 390.90%, 68.94%, 224.43%, 16.19%, and 224.40% higher than those of PLA/PBAT composite, respectively.Highlights PLA grafted GND with a single epoxy group is prepared by solid phase grafting. PLA-GND as a non-reactive compatibilizer compatibilizes PLA/PBAT composite. The similar chain of GND and PBAT is helpful to form the physical entanglement. The physical entanglement is essential to improve compatibility of PLA and PBAT. PLA/PBAT composite has excellent overall performance at a PLA-GND content of 5 wt%. Schematic diagram of compatibilization effect of non-reactive compatibilizer PLA-GND on PLA/PBAT composite. image
Keyword ：
compatibilization compatibilization non-reactive compatibilizer non-reactive compatibilizer PLA/PBAT composite PLA/PBAT composite poly(lactic acid) grafted glycidyl neodecanoate poly(lactic acid) grafted glycidyl neodecanoate solid phase grafting solid phase grafting
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| GB/T 7714 | Chen, Xiaoting , Chen, Enzhao , Wu, Kangdi et al. Preparation of poly(lactic acid) grafted glycidyl neodecanoate by solid phase grafting and its compatibilization for poly(lactic acid)/poly(butylene adipate-co-terephthalate) composite [J]. | POLYMER ENGINEERING AND SCIENCE , 2024 , 64 (9) : 4099-4111 . |
| MLA | Chen, Xiaoting et al. "Preparation of poly(lactic acid) grafted glycidyl neodecanoate by solid phase grafting and its compatibilization for poly(lactic acid)/poly(butylene adipate-co-terephthalate) composite" . | POLYMER ENGINEERING AND SCIENCE 64 . 9 (2024) : 4099-4111 . |
| APA | Chen, Xiaoting , Chen, Enzhao , Wu, Kangdi , Li, Tianze , Teng, Guanqi , Li, Baoming . Preparation of poly(lactic acid) grafted glycidyl neodecanoate by solid phase grafting and its compatibilization for poly(lactic acid)/poly(butylene adipate-co-terephthalate) composite . | POLYMER ENGINEERING AND SCIENCE , 2024 , 64 (9) , 4099-4111 . |
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Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide (MoS2-RGO@AO7-PEDOT) composite is prepared via a facile two-step approach, where the first step is the molybdenum disulfide (MoS2) nanosheets dispersing on reduced graphene oxide (RGO) evenly using a hydrothermal method, and the second step involves the stable coating of acid orange 7 (AO7) doped poly(3,4-ethylenedioxythiophene) (PEDOT) on the MoS2-RGO surface through chemical oxidation method with AO7 acting as a guide and connector. At a mass ratio of 4:1 between 3,4-ethylenedioxythiophene (EDOT) and MoS2-RGO, MoS2-RGO is coated by AO7 doped PEDOT, and the composite shows a discontinuous lamellar structure without agglomeration of PEDOT, which provides a significant interface between the composite and the electrolyte in favor of increasing the contact area. The large contact area is beneficial for active substances to participate in the redox reaction for charge storage and improving the ion transport efficiency of the electrolyte, which would lead to enhanced electrochemical performance. The composite's specific capacitance in 1 mol L-1 sulfuric acid (H2SO4) is 233 F g-1, which surpasses that of PEDOT by 101%, and the composite retains an impressive 70.6% of its initial specific capacitance after 10,000 cycles. In addition, a flexible all-solid-state supercapacitor is created to investigate its practical application, where H2SO4/polyvinyl alcohol is utilized as the ionic electrolyte and spacer. The supercapacitor demonstrates a maximum energy density of 7.2 Wh kg-1 at a power density of 600 W kg-1, and it maintains 3.52 Wh kg-1 even under high-power density of 4800 W kg-1.
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| GB/T 7714 | Wang, Yasen , Jiang, Junhui , Li, Baoming . Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide composite as an electrode material for flexible all-solid-state supercapacitors [J]. | JOURNAL OF MATERIALS SCIENCE , 2024 , 59 (5) : 2055-2069 . |
| MLA | Wang, Yasen et al. "Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide composite as an electrode material for flexible all-solid-state supercapacitors" . | JOURNAL OF MATERIALS SCIENCE 59 . 5 (2024) : 2055-2069 . |
| APA | Wang, Yasen , Jiang, Junhui , Li, Baoming . Acid orange 7 doped poly(3,4-ethylenedioxythiophene)/molybdenum disulfide/reduced graphene oxide composite as an electrode material for flexible all-solid-state supercapacitors . | JOURNAL OF MATERIALS SCIENCE , 2024 , 59 (5) , 2055-2069 . |
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The overexpression of microRNA-222 (miRNA-222) is closely related to many human diseases, so the development of biosensors to detect this biomarker will contribute to the diagnosis of related diseases. Here, a simple, sensitive and specific fluorescence assay for the detection of miRNA-222 was developed using red-emitting upconversion nanoparticle (UCNP) as the donor and a DNA hairpin with black hole quencher-2 (BHQ-2) as the acceptor. Li+ and Tm3+-doped UCNP with a strong emission peak at 654 nm was obtained by changing the doped ion ratio and constructing core-shell structures. Under optimal conditions, the linear range for detecting miRNA-222 is 0.5-2.5 nM and the limit of detection is as low as 0.077 nM without any complicated amplification strategy. Finally, the proposed assay was applied for the detection of miRNA-222 in serum samples. The results obtained were similar to those of the standard method, and the spiked recoveries were in the range of 97.62%- 102.14 %, suggesting that the proposed method has practical value in a complex biological sample matrix.
Keyword ：
DNA-Functionalized DNA-Functionalized miRNA miRNA Red-emitting Red-emitting UCNP UCNP
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| GB/T 7714 | Li, Yingchao , Tu, Canzhao , Chen, Qianshun et al. Enhanced red emission of upconversion nanoparticles via Li+ and Tm3+codoping and active core-shell construction for sensitive detection of miRNAs [J]. | ANALYTICA CHIMICA ACTA , 2024 , 1335 . |
| MLA | Li, Yingchao et al. "Enhanced red emission of upconversion nanoparticles via Li+ and Tm3+codoping and active core-shell construction for sensitive detection of miRNAs" . | ANALYTICA CHIMICA ACTA 1335 (2024) . |
| APA | Li, Yingchao , Tu, Canzhao , Chen, Qianshun , Lin, Yingying , Li, Baoming , Lyu, Haixia . Enhanced red emission of upconversion nanoparticles via Li+ and Tm3+codoping and active core-shell construction for sensitive detection of miRNAs . | ANALYTICA CHIMICA ACTA , 2024 , 1335 . |
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本发明公开了一种基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法，属于食品添加剂的检测技术领域。所述检测方法是先利用表面配体交换反应制备柠檬酸钠修饰核壳结构上转换纳米粒子，再通过超声作用制备二氧化锰纳米片修饰核壳结构上转换纳米粒子，最后，绘制“荧光强度变化比率‑叔丁基对苯二酚浓度”标准工作曲线，建立线性工作方程。本发明检测方法能够实现对水溶液中食品添加剂叔丁基对苯二酚的检测，且具有线性检测范围宽、检测限低、灵敏度高等优势，在食品和环境领域具有广泛的应用前景。
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| GB/T 7714 | 李宝铭 , 林莹莹 , 邢益锋 et al. 基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法 : CN202111395473.2[P]. | 2021-11-23 00:00:00 . |
| MLA | 李宝铭 et al. "基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法" : CN202111395473.2. | 2021-11-23 00:00:00 . |
| APA | 李宝铭 , 林莹莹 , 邢益锋 , 吕海霞 . 基于核壳结构上转换纳米粒子检测叔丁基对苯二酚的方法 : CN202111395473.2. | 2021-11-23 00:00:00 . |
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本发明公开了一种非反应性增容PLA/PBAT复合材料及其制备方法，属于高分子复合材料的制备技术领域。所述复合材料是以聚乳酸为原料，以聚己二酸对苯二甲酸丁二酯为增韧剂，以固相接枝法制得的聚乳酸接枝新癸酸缩水甘油酯为增容剂，经熔融共混制备而成。本发明制得的复合材料具有较高的拉伸强度、较优异的韧性、较低的熔体黏度和可完全生物降解性，主要用于医疗、服饰、汽车、食品包装领域，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 吴康迪 , 王静 et al. 一种非反应性增容PLA/PBAT复合材料及其制备方法 : CN202211212070.4[P]. | 2022-09-30 00:00:00 . |
| MLA | 李宝铭 et al. "一种非反应性增容PLA/PBAT复合材料及其制备方法" : CN202211212070.4. | 2022-09-30 00:00:00 . |
| APA | 李宝铭 , 吴康迪 , 王静 , 张璇 . 一种非反应性增容PLA/PBAT复合材料及其制备方法 : CN202211212070.4. | 2022-09-30 00:00:00 . |
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本发明公开了一种抗湿滑改性热塑性聚氨酯及其制备方法和应用，属于热塑性聚氨酯抗湿滑改性技术领域。所述抗湿滑改性热塑性聚氨酯是以热塑性聚氨酯为基体，以非硫化溴化丁基橡胶为抗湿滑改性剂，以γ‑氨丙基三乙氧基硅烷为相容剂，以硬脂酸锌为热稳定剂，以棕榈油为增塑软化剂，经熔融共混制备而成。本发明制得的抗湿滑改性热塑性聚氨酯具有较高的干、湿摩擦系数、较大的拉伸强度和断裂伸长率、较低的硬度，主要用于制作运动鞋、安全鞋的鞋底，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 林海峰 , 陶涛 et al. 一种抗湿滑改性热塑性聚氨酯及其制备方法和应用 : CN202210461947.7[P]. | 2022-04-29 00:00:00 . |
| MLA | 李宝铭 et al. "一种抗湿滑改性热塑性聚氨酯及其制备方法和应用" : CN202210461947.7. | 2022-04-29 00:00:00 . |
| APA | 李宝铭 , 林海峰 , 陶涛 , 熊雷 . 一种抗湿滑改性热塑性聚氨酯及其制备方法和应用 : CN202210461947.7. | 2022-04-29 00:00:00 . |
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本发明公开了一种高韧性耐热聚乳酸复合材料及其制备方法，属于聚乳酸改性技术领域。所述高韧性耐热聚乳酸复合材料是以聚乳酸为基体，蒙脱土接枝丙交酯为填充剂，聚对苯二甲酸丁二酸丁二酯为增韧剂，以熔融接枝法制备的甲基丙烯酸缩水甘油酯和甲基丙烯酸丁酯共接枝聚乳酸为相容剂，癸二酸二苯基二酰肼为成核剂，经熔融共混制备而成。本发明制得的聚乳酸复合材料具有较低的原料成本、较高的韧性和热变形温度以及可完全生物降解性，适用于医疗、服饰、汽车、食品包装等领域，具有显著的经济价值与社会效益。
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| GB/T 7714 | 李宝铭 , 陶涛 , 林海峰 et al. 一种高韧性耐热聚乳酸复合材料及其制备方法 : CN202211428488.9[P]. | 2022-11-15 00:00:00 . |
| MLA | 李宝铭 et al. "一种高韧性耐热聚乳酸复合材料及其制备方法" : CN202211428488.9. | 2022-11-15 00:00:00 . |
| APA | 李宝铭 , 陶涛 , 林海峰 , 熊雷 . 一种高韧性耐热聚乳酸复合材料及其制备方法 : CN202211428488.9. | 2022-11-15 00:00:00 . |
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Congo red doped poly (3,4-ethylene dioxythiophene)/graphene oxide (GO/CR-PEDOT) composite was prepared by simple chemical oxidation method, where Congo red doped poly (3,4-ethylene dioxythiophene) (CR-PEDOT) evenly and stably coated on the surface of graphene oxide (GO) under the guidance and connection of congo red (CR), respectively. Therefore, GO with a large specific surface area could bring into full play its function as a supporting skeleton to decrease the degree of volume expansion and shrinkage of GO/CR-PEDOT composite in charge/discharge process and improve its specific capacitance and cycle stability. The results showed that the maximum specific capacitance of GO/CR-PEDOT composite was up to 227 F/g when the feeding mass ratio of GO to 3,4-ethylene dioxythiophene was 1:1, which was 110% higher than that of poly (3,4-ethylene dioxythiophene) (PEDOT), and the capacitance retention was 92.3 % after 10,000 cycles. Furthermore, a model of asymmetric supercapacitor was fabricated by using GO/CR-PEDOT composite as positive material, activated carbon as negative material and 1 mol/L Na2SO4 as electrolyte, which exhibited that the energy density was as high as 14.4 Wh/kg when the power density was 996 W/kg and still achieved 9.11 Wh/kg at a high power density of 7999 W/kg. (C) 2021 Elsevier Ltd. All rights reserved.
Keyword ：
Asymmetric supercapacitor Asymmetric supercapacitor Congo red Congo red Graphene oxide Graphene oxide Poly (3,4-ethylene dioxythiophene) Poly (3,4-ethylene dioxythiophene)
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| GB/T 7714 | Du, Yuanyuan , Cao, Dingfa , Li, Baoming et al. Stable conge red doped poly (3,4-ethylene dioxythiophene)/graphene oxide composite as electrode material for high-performance asymmetric supercapacitors [J]. | ELECTROCHIMICA ACTA , 2021 , 395 . |
| MLA | Du, Yuanyuan et al. "Stable conge red doped poly (3,4-ethylene dioxythiophene)/graphene oxide composite as electrode material for high-performance asymmetric supercapacitors" . | ELECTROCHIMICA ACTA 395 (2021) . |
| APA | Du, Yuanyuan , Cao, Dingfa , Li, Baoming , Lu, Haixia , Shen, Yu . Stable conge red doped poly (3,4-ethylene dioxythiophene)/graphene oxide composite as electrode material for high-performance asymmetric supercapacitors . | ELECTROCHIMICA ACTA , 2021 , 395 . |
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