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In this study, we combined the traditional vacuum furnace with a sur-high accuracy vacuum gauge for measuring the change of gas pressure in the furnace as a function of temperature. The modified vacuum furnace was used for preparing silicon carbide (SiC), and the recorded data named thermobarogram were applied to detect the reaction temperature for synthesis of SiC, which, in particular, changes as catalysts are used. The results showed that the carbothermal reduction temperature for synthesizing SiC, under dynamic vacuum condition, would decrease to 850 degrees C when the mole ratio of Fe/Si = 0.06 was employed in the SiC precursor. (C) 2007 Elsevier Ltd. All rights reserved.
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VACUUM
ISSN: 0042-207X
Year: 2007
Issue: 3
Volume: 82
Page: 336-339
0 . 8 8 1
JCR@2007
3 . 8 0 0
JCR@2023
ESI Discipline: MATERIALS SCIENCE;
JCR Journal Grade:3
Cited Count:
SCOPUS Cited Count: 5
ESI Highly Cited Papers on the List: 0 Unfold All
WanFang Cited Count:
Chinese Cited Count:
30 Days PV: 1
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