Synthesis of dihydropyrazole-bridged dinuclear ferrocenyl derivatives and their catalytic effect on thermal decomposition of ammonium perchlorate - Details

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Abstract：

Dihydropyrazole-bridged　dinuclear　ferrocenyl　derivatives　(3a-3c)　have　been　synthesized　by　the　reaction　of　1,3-diferrocenyl-2-propen-1-on　(1)　with　hydrazine,　then　acylation　with　acyl　chloride　directly.　The　structures　were　determined　by　mass　spectrometry,　IR　and　1H　NMR　spectroscopy.　The　compound　3c　was　characterized　by　single-crystal　X-ray　analyses.　It　was　found　that　compounds　3a-3c　have　significant　catalytic　effect　on　the　decomposition　of　ammonium　perchlorate　(AP).　Compared　with　the　thermal　decomposition　of　pure　AP,　adding　3a,　3b　and　3c　in　AP　decreases　its　decomposition　temperature　by　78.8,　74.3　and　57.1　°C,　respectively.　©　2011　John　Wiley　&　Sons,　Ltd.

Keyword：

Chlorine compounds Decomposition Inorganic compounds Iron compounds Mass spectrometry Nitrogen compounds Nuclear magnetic resonance spectroscopy Organometallics Pyrolysis Single crystals Thermolysis

Community：

[ 1 ] [Gao, Yong]Department of Chemistry, Fuzhou University, Fuzhou 350108, China
[ 2 ] [Gao, Yong]College of Chemistry and Materials Science, Fujian Normal University, Fuzhou 350007, China
[ 3 ] [Li, Heng-Dong]Department of Chemistry, Fuzhou University, Fuzhou 350108, China
[ 4 ] [Li, Heng-Dong]State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 5 ] [Ke, Cheng-Feng]Department of Chemistry, Fuzhou University, Fuzhou 350108, China
[ 6 ] [Ke, Cheng-Feng]State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 7 ] [Xie, Li-Li]Department of Chemistry, Fuzhou University, Fuzhou 350108, China
[ 8 ] [Xie, Li-Li]State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 9 ] [Wei, Bing]Department of Chemistry, Fuzhou University, Fuzhou 350108, China
[ 10 ] [Wei, Bing]State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou 350002, China
[ 11 ] [Yuan, Yao-Feng]Department of Chemistry, Fuzhou University, Fuzhou 350108, China
[ 12 ] [Yuan, Yao-Feng]State Key Laboratory Breeding Base of Photocatalysis, Fuzhou University, Fuzhou 350002, China

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yaofeng_yuan@fzu.edu.cn

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Source ：

Applied Organometallic Chemistry

ISSN： 0268-2605

Year： 2011

Issue： 6

Volume： 25

Page： 407-411

2 . 0 6 1

JCR@2011

3 . 7 0 0

JCR@2023

JCR Journal Grade：2

CAS Journal Grade：3

Cited Count：

WoS CC Cited Count：

SCOPUS Cited Count： 33

ESI Highly Cited Papers on the List： 0 Unfold All

WanFang Cited Count：

Chinese Cited Count：

30 Days PV： 1

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