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Microwave dielectric ceramics of CaLa4Ti4O15 were prepared by the solid-state reaction method. The influence of the calcining temperature on the sintering behavior and microwave dielectric properties was investigated. For the specimen calcined at 1200C, CaTiO3, La2Ti2O7 and La2TiO5 mixed phases were observed in addition to the CaLa4Ti4O15 phase, while the hexagonal perovskite single phase was achieved for the CaLa4Ti4O15 powders calcined at 1300C or 1400C. CaLa4Ti4O15 ceramics were sintered well with high relative density of about 97%. On the other hand, the ceramics had a high mechanical quality factor plus resonant frequency (Q × f) value and near zero temperature coefficient of resonant frequency (τf). The CaLa4Ti4O15 ceramics sintered at 1550C exhibited excellent microwave dielectric properties as follows: relative dielectric constant Εr =45.1, Q × f =46 087 GHz, τf = -14.1 × 10-6/°C and Εr =45.9, Q × f =48 871 GHz, τf = -14.4 × 10-6/°C for the specimens calcined at 1200C and 1300C, respectively.
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Journal of the Chinese Ceramic Society
ISSN: 0454-5648
CN: 11-2310/TQ
Year: 2008
Issue: 12
Volume: 36
Page: 1695-1699
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 2
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