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标题化合物是由[Ni(bipy)3]2+络合物与FeCl2在MeOH、 DMF及异丙醇混合溶剂中直接反应得到的, 它可溶于水、乙醇和DMF等极性溶剂, 不溶于乙醚. X-射线结晶学研究表明: 标题物中含有[Ni(bipy)3]2+和[(μ-oxo)Fe2Cl6]2-离子, 晶胞参数: 单斜, P21/c, a=0.9709nm, b=2.6409nm, c=1.4014nm, β=100.24°, V=3.536nm3, Z=4, D\-c=1.630g/cm\+3, F(000)=1744, μ=1.824nm-1. 化学实验式为: C30H24Cl\-6Fe\-2N\-6NiO. 分子量Mr=867.66. 对标题物进行X-荧光元素分析、红外、可见吸收光谱和磁化率的研究.
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福州大学学报(自然科学版)
ISSN: 1000-2243
CN: 35-1337/N
Year: 2002
Issue: 5
Volume: 30
Page: 618-619,631
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ESI Highly Cited Papers on the List: 0 Unfold All
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30 Days PV: 0
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