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author:

Zheng, Y. (Zheng, Y..) [1] | Rao, F. (Rao, F..) [2] | Yang, L. (Yang, L..) [3] | Zhong, S. (Zhong, S..) [4]

Indexed by:

Scopus

Abstract:

In this study, combined waste-derived alkali activators are used to prepare volcanic ash-based geopolymers and to evaluate their durability under freeze–thaw conditions. The comparable alkali activators are Na2SO4–Ca(OH)2 (N–C), Na2SO4-calcium carbide residue (N-CCR), Na2SO4-calcium carbide residue-NaOH (N-CCR-H), Na2SO4-calcium carbide residue-Na2SiO3 (N-CCR-S). Microstructure and strength of the geopolymers are characterized through XRD, SEM, FTIR, NMR and compressive strength measurements. Pore structure of the geopolymers is determined by adsorption/desorption isotherms and BET calculations. It is found that the ternary alkali activators give superior activation synergy than dual alkali activators. The compressive strengths of N-CCR-S and N-CCR geopolymers are 61.0 MPa and 23.1 MPa after 7 d in air. After freeze–thaw cycles for 30 days, the compressive strength of the N-CCR-S geopolymer is three times higher than that of the N-CCR geopolymer. These significant differences originate from their N-A-S-H and C-(A)-S-H gel structures. The N-CCR-S geopolymers possess a more homogeneous and dense microstructure with low pore structure. This study proposes a method for the effective utilization of volcanic ash and alkaline solid wastes. © 2022 Elsevier Ltd

Keyword:

Calcium carbide residue Freeze–thaw cycles Gel structure Geopolymers Volcanic ash

Community:

  • [ 1 ] [Zheng, Y.]School of Materials Science and Engineering, Fuzhou University, Fujian, Fuzhou, 350108, China
  • [ 2 ] [Rao, F.]School of Materials Science and Engineering, Fuzhou University, Fujian, Fuzhou, 350108, China
  • [ 3 ] [Rao, F.]Zijin School of Geology and Mining, Fuzhou University, Fujian, Fuzhou, 350108, China
  • [ 4 ] [Yang, L.]Zijin School of Geology and Mining, Fuzhou University, Fujian, Fuzhou, 350108, China
  • [ 5 ] [Yang, L.]Fujian Key Laboratory of Green Extraction and High-value Utilization of Energy Metals, Fuzhou University, Fujian, Fuzhou, 350108, China
  • [ 6 ] [Zhong, S.]School of Materials Science and Engineering, Fuzhou University, Fujian, Fuzhou, 350108, China
  • [ 7 ] [Zhong, S.]Zijin School of Geology and Mining, Fuzhou University, Fujian, Fuzhou, 350108, China

Reprint 's Address:

  • [Rao, F.]School of Materials Science and Engineering, Fujian, China;;[Yang, L.]School of Materials Science and Engineering, Fujian, China

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Related Keywords:

Source :

Cement and Concrete Composites

ISSN: 0958-9465

Year: 2023

Volume: 136

1 0 . 8

JCR@2023

1 0 . 8 0 0

JCR@2023

ESI HC Threshold:49

JCR Journal Grade:1

CAS Journal Grade:1

Cited Count:

WoS CC Cited Count: 0

SCOPUS Cited Count: 16

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 2

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