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author:

Li Xiang-hui (Li Xiang-hui.) [1] | Yang Fang (Yang Fang.) [2] | Lin Zhen-yu (Lin Zhen-yu.) [3] (Scholars:林振宇) | Qiu Bin (Qiu Bin.) [4] (Scholars:邱彬) | Wang Dan-hong (Wang Dan-hong.) [5]

Indexed by:

EI Scopus SCIE PKU CSCD

Abstract:

Based on the initial near-infrared spectrum of edible essence samples and its mixture with DEHP and DINP, we chose the wavelength ranges of 8 800 similar to 8 540 and 7 500 similar to 5 085 cm(-1) to use the principal component analysis (PCA) method to distinguish these three types of samples. The correct rate of the identification is proved to be 100%. Meanwhile, we measured the content of DEHP and DINP (with the concentration ranging between 0 and 100 mg . kg(-1)) in the edible essence and established the quantitative analysis model by using partial least squares (PLS). It was found that the relative errors of the prediction results of DEHP and DINP are -1.23%similar to 3% and -1%similar to 3.6%, respectively, and the relative root-mean-square errors of prediction (RRMSEP) of them are 1.39 and 0.98, respectively. This study provides a simple, rapid and accurate method to detect the additive dosage of plasticizing agents in edible essence in the food industry.

Keyword:

Cluster analysis (CA) Near-infrared spectrum (NIRS) Partial least-squares (PLS) Plasticizer Principal component analysis (PCA)

Community:

  • [ 1 ] [Li Xiang-hui]Fuzhou Univ, MOE Key Lab Anal & Detect Food Safety, Fujian Prov Key Lab Anal & Detect Technol Food Sa, Dept Chem, Fuzhou 350108, Peoples R China
  • [ 2 ] [Lin Zhen-yu]Fuzhou Univ, MOE Key Lab Anal & Detect Food Safety, Fujian Prov Key Lab Anal & Detect Technol Food Sa, Dept Chem, Fuzhou 350108, Peoples R China
  • [ 3 ] [Qiu Bin]Fuzhou Univ, MOE Key Lab Anal & Detect Food Safety, Fujian Prov Key Lab Anal & Detect Technol Food Sa, Dept Chem, Fuzhou 350108, Peoples R China
  • [ 4 ] [Yang Fang]Fujian Entry Exit Inspect & Quarantine Bur PRC, Fuzhou 350001, Peoples R China
  • [ 5 ] [Wang Dan-hong]Fujian Entry Exit Inspect & Quarantine Bur PRC, Fuzhou 350001, Peoples R China

Reprint 's Address:

  • [Yang Fang]Fujian Entry Exit Inspect & Quarantine Bur PRC, Fuzhou 350001, Peoples R China

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Source :

SPECTROSCOPY AND SPECTRAL ANALYSIS

ISSN: 1000-0593

CN: 11-2200/O4

Year: 2013

Issue: 3

Volume: 33

Page: 690-693

0 . 2 7

JCR@2013

0 . 7 0 0

JCR@2023

ESI Discipline: CHEMISTRY;

JCR Journal Grade:4

CAS Journal Grade:4

Cited Count:

WoS CC Cited Count: 2

SCOPUS Cited Count: 2

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 3

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