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author:

Wu, WS (Wu, WS.) [1] | Liu, SX (Liu, SX.) [2]

Indexed by:

Scopus SCIE PKU CSCD

Abstract:

The title compound C9H11N3O2 has been synthesized. The crystal belongs to the monoclinic system, space group C2/c with cell parameters: a=13.703(1), b=9.142(1), c=16.437(2) Angstrom, beta =105.547(3)degrees, V=1983.8(4)Angstrom (3), Z=8, D-c=1.294g/cm(3), M-r=193.21, F(000)= 816, mu (MoKalpha)=0.094 mm(-1). Final R and wR are 0.0527 and 0.1517, respectively for 1596 [I greater than or equal to2 sigma (I)] observed reflections. There are intermolecular hydrogen bonds in the crystal. The network structure was formed through the intermolecular hydrogen bonds. The hydrogen bond lengths of N(2)-H . . .N (1a)(a: -x+1, y, -z+1/2) and N(3)-H . . .O(2b)(b: -x+1/2, y-1/2, -z+1/2) are 3.007(2) and 2.786(2)Angstrom respectively.

Keyword:

crystal structure dihydrazide synthesis

Community:

  • [ 1 ] Fuzhou Univ, Cent Lab, Fuzhou 350002, Peoples R China
  • [ 2 ] Huaqiao Univ, Coll Mat, Quanzhou 362011, Peoples R China

Reprint 's Address:

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    [Wu, WS]Fuzhou Univ, Cent Lab, Fuzhou 350002, Peoples R China

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Source :

CHINESE JOURNAL OF STRUCTURAL CHEMISTRY

ISSN: 0254-5861

CN: 35-1112/TQ

Year: 2001

Issue: 3

Volume: 20

Page: 226-228

0 . 1 8 4

JCR@2001

5 . 9 0 0

JCR@2023

ESI Discipline: CHEMISTRY;

JCR Journal Grade:4

Cited Count:

WoS CC Cited Count: 13

SCOPUS Cited Count:

ESI Highly Cited Papers on the List: 0 Unfold All

WanFang Cited Count:

Chinese Cited Count:

30 Days PV: 0

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